sodium chloride solubility in tetrahydrofuran

Liu Y, Mellmer MA, Alonso DM, Dumesic JA. It was discovered by Finholt, Bond and Schlesinger in 1947. Epub 2015 Apr 27. Effect of Tetrahydrofuran on the Solubilization and Depolymerization of Cellulose in a Biphasic System. Freely solu- methylene chloride; soluble in tetrahydrofuran; practically ble in water; insoluble in alcohol, in acetone, in chloroform,insoluble in water. - Ch.1. – P. 189 • Seidell A. Solubilities of inorganic and metal organic compounds. A solubility equation was proposed and verified by experimental results. Promoting Effect of Sodium Chloride on the Solubilization and Depolymerization of Cellulose from Raw Biomass Materials in Water. * Tetrahydrofuran may damage the liver and kidneys.  |  The ion–dipole interactions between Li + ions and acetone molecules in a solution of LiCl in acetone are shown in … Solubility Absorption Application(s) Additive pH Value Physical Form UV-Absorption Values Special Grade. TETRAHYDROFURAN 1. - pod red. To find more Sodium chloride information like chemical properties, structure, melting point, boiling point, density, molecular formula, molecular weight, physical properties and toxicity information. NLM National Center for Biotechnology Information, Unable to load your collection due to an error, Unable to load your delegates due to an error. Author information: (1)Key Laboratory of Green Chemistry and Technology, Ministry of Education, College of Chemistry, Sichuan University, Chengdu, Sichuan, 610064, China. Tetrahydrofuran (THF), or oxolane, is an organic compound with the formula (CH 2) 4 O. - M.: Nauka, 1986. – P. 77 • Grinvud N., Ernsho A. Himiya elementov. Tehnologiya mineral'nyh soley (udobreniy, pesticidov, promyshlennyh soley, okislov i kislot). Pletenevoy T.V. – P. 38 • Furman A.A. Neorganicheskie hloridy (himiya i tehnologiya). – P. 299 • Devyatkin V.V., Lyahova Yu.M. – P. 27 • Himicheskaya tehnologiya neorganicheskih veschestv. - T.2. neat Melting Point: 220°C -neat Specific Gravity: 0.902 Vapor Pressure, 15°: 144mm-THF Vapor Density (air=1): 2.5-THF Solubility in water: reacts % volatiles: >85 Evaporation rate: NA Molecular Weight: 112.21 Other: NA Inorganic Compound; Flavouring Agent; Food Additive Toxin, Toxin-Target Database T3D4666: ORL-RAT LD50 3000 mg kg-1 , ORL-MUS LD50 4000 mg kg-1 , IPR-MUS LD50 2602 mg kg-1 , ICV-MUS LD50 131 mg kg-1 , SKN-RBT LD50 > 10000 mg kg-1 OU Chemical Safety Data (No longer updated) More details - Yaroslavl': Akademiya Holding, 2000. 2010;290:311-39. doi: 10.1007/128_2008_35. Laboratoriya znaniy, 2008. Jiang Z(1), Zhao P(1), Li J(1), Liu X(1), Hu C(1). In the NaCl-H2 O-THF system, THF could significantly promote the effects of both H2 O and NaCl on the disruption of O2-H⋅⋅⋅O6 and O3-H⋅⋅⋅O5 intramolecular hydrogen bonds, respectively. Keywords: Sodium hydroxide 1%: LDPE at 20°C-50°C: shows little or no damage after 30 days. - t.5. Nearly half of the O6-H⋅⋅⋅O3 intermolecular hydrogen bonds could be broken by THF in the H2 O-THF co-solvent system, whereas the cleavage of O2-H⋅⋅⋅O6 intramolecular hydrogen bonds by H2 O was significantly inhibited. 1.0 g/cm3 at 20 °C Water solubility (Not applicable) Molecular weight 88.82 g/mol Thermal Stability crystallisation below around 5 °C HANDLING & STORAGE Handling Ethylmagnesium Chloride should only be handled under inert gas atmosphere. solubility of sodium citrate . - M.: Medicina, 1979. - M.-L.: Himiya, 1965. - M.: BINOM.  |  Front Chem. Polar solvents are hydrophilic but non-polar solvents are lipophilic. Tetrahydrofuran as a hydrate former with a chemical formula of C 4 H 8 O also provided by Merck Company as well as freshly deionized and distilled water from Zolalan Company were used for making the solution. - M.: BINOM. Effects of Water on the Copper-Catalyzed Conversion of Hydroxymethylfurfural in Tetrahydrofuran. Sodium chloride, saturated: LDPE / HDPE at 20°C-50°C: little or no damage after 30 days. PVC (Polyvinyl chloride) Chemical Compatibility Chart: Check the chemical compatibility of Polyvinyl chloride / PVC with various chemicals, solvents, alcohols and other products.. Shop PVC. The freezing point is −21.12 °C for 23.31 wt% of salt, and the boiling point of saturated salt solution is near 108.7 °C. Himicheskoe ravnovesie. Freely soluble in water, in methanol, in alcohol, and in dimethylformamide; sparingly soluble in dehydrated alcohol; practically insoluble in isopropyl alcohol, in butyl alcohol, and in acetone. Mostofian B, Cai CM, Smith MD, Petridis L, Cheng X, Wyman CE, Smith JC. Very high exposure can cause unconsciousness and death. 2H 2 O (MW 225.63) Alternate Name: tin(II) chloride dihydrate. As a cheap and reusable system, NaCl-H2 O-THF system may be a promising approach for the dissolution and further conversion of cellulose in lignocellulosic biomass without any enzymes, ionic liquids, or conventional catalysts. Oil and water don't mix but separate into two layers. 1961]. - M.: Sovetskaya enciklopediya, 1992. HCl ) : White to light yellow powder. Leave A Message – P. 1217-1249 • Belikov V.G. Please enable it to take advantage of the complete set of features! Please Note: The information in this chart has been supplied by reputable sources and is to be used ONLY as a guide in selecting equipment for appropriate chemical compatibility. Laboratoriya znaniy, 2008. 66 °C (Tetrahydrofuran) Density ca. In addition, THF could protect and transfer the cellulose-derived products to the organic phase by forming hydrogen bonds between the oxygen atom in THF and the hydrogen atom of C4-OH in the glucose or aldehyde group in 5-hydroxymethylfurfural (HMF), which can lead more NaCl to combine with the -OH of M-cellulose and further disrupt hydrogen bonding in M-cellulose, thereby improving the yield of small molecular weight products (especially HMF) and further promoting the dissolution of cellulose. The dissolution of cellulose from biomass is a crucial but complicated issue for maximizing the utilization of biomass resources to produce valuable chemicals, because of the extreme insolubility of cellulose. USA.gov. Sodium chloride is stable. - M.: Vysshaya shkola, 2002. It was found that the hydrate promoting effect of tetrahydrofuran is able to suppress the inhibiting effect of sodium chloride especially at lower concentration of sodium chloride. - T.3. The compound is classified as heterocyclic compound, specifically a cyclic ether.It is a colorless, water-miscible organic liquid with low viscosity.It is mainly used as a precursor to polymers. - T.1. - pod red. tens. SOLUBILITY:1-butanol [C4H9OH]: 0,005 (20°), 1-hexanol [C6H14O]: 0,001 (20°)1-pentanol [CH3CH2CH2CH2CH2OH]: 0,002 (20°)2-butanol [CH3CH(OH)CH2CH3]: 0,00047 (25°), 2-ethylhexanol [C8H18O]: 0,0001 (20°)ammonia liquid [NH3]: 4,2 (-30°), 12,9 (0°)acetone [(CH3)2CO]: 0,000032 (18°)benzalcohol [C6H5CH2OH]: 0,017 (20°)water [H2O]: 35,7 (0°), 35,9 (20°), 36,4 (40°), 37,2 (60°), 38,1 (80°), 39,4 (100°), heavy water [D2O]: 29,2 (0°), 33,9 (100°)hydrazine [N2H4]: 8 (20°)hydroxylamine [NH2OH]: 14,7 (17,5°)glycerol [HOCH2CH(OH)CH2OH]: 8,2 (25°)sulfur dioxide [SO2]: 0,016 (0°)diethyl ether [C2H5OC2H5]: solventlessisoamil alcohol [C5H11OH]: 0,0016 (20°)isobutanol [(CH3)2CHCH2OH]: 0,0005 (20°)isopropyl alcohol [CH3CH(OH)CH3]: 0,0027 (25°)methanol [CH3OH]: 1,31 (25°)formic acid [HCO2H] 95%: 5,8 (19,7°)hydrogen peroxide [H2O2]: 17,6 (-14,5°), 18,4 (-10°), 20,5 (0°)propanol [(CH3)2CHOH]: 0,012 (25°)selenium (iv) oxide-dichloride [SeOCl2]: 0,57 (25°)phosphoryl chloride [POСl3]: 0,018acetic acid [CH3COOH]: 0,074 (30°)ethanol [C2H5OH] abs. Polarity has a direct effect on solubility (and miscibility). The solubility of a substance is the maximum amount of a solute that ... 37.5 g of NaCl, and 4.8 g of NaF. Storax: Semiliquid, grayish to grayish-brown, sticky, opaque mass depositing on standing a heavy dark brown layer (Levant Storax); or semisolid, sometimes a solid mass, softened by gently warming (American Storax). Using potassium hydroxide or sodium hydroxide to dry impure Tetrahydrofuran that contains peroxides has resulted in explosions. The interaction of water with Na + and Cl − ions in an aqueous solution of NaCl was illustrated in Figure 4.3 "The Dissolution of Sodium Chloride in Water". – P. 33-43. - 3ed., vol.1 - New York: D. Van Nostrand Company, 1940. Avoid contact with eyes, skin and clothes as well as inhalation. – P. 289-302 • Spravochnik himika. Ahmetova T.G., kn.1. HAZARDS IDENTIFICATION ... and Sodium Aluminum Hydride, Potassium hydroxide, Calcium Hydride. lizing agent. NIH Local Phase Separation of Co-solvents Enhances Pretreatment of Biomass for Bioenergy Applications. – P. 36 • Novyy spravochnik himika i tehnologa.  |  The solubilities of citric, malic and malonic acids in ethanol, 1,4-dioxane, water, acetonitrile, 2-propanol, and tetrahydrofuran (THF) were measured over the temperature range of 303.2–333.2K. Physical properties about Sodium chloride are: Water solution of Sodium chloride is alkaline with the PH value 6.7-7.3. – P. 10-18 • Himicheskaya enciklopediya. In this work, the competing effects of sodium chloride (NaCl) and tetrahydrofuran (THF) on carbon dioxide hydrate formation are investigated through phase equilibrium measurements. Is transparent in thin layers, has a characteristic odor and taste, and is more dense than water. News 39(40):57. Would you like email updates of new search results? – P. 86 • Toksikologicheskiy vestnik. – P. 239 • Pozin M.E. - L.: Himiya, 1977. - T.1. - 2004. – P. 602 610 • Spravochnik himika. Eng. Solubility: varying solubility in water, methanol, ethanol, tetrahydrofuran… - L.: Himiya, 1988. Non-polar solvents dissolve non-polar compounds best. Sodium chloride will become corrosive to metals when wet. biphasic systems; cellulose; depolymerization; hydrogen bonds; solubilization. : 0,065 (18,5°)ethylene glycol [HOCH2CH2OH]: 46,4 (1,8°)PROPERTIES:colourless cubic crystalsM (molar mass): 58,440 g/molMP (melting point): 801 °CMB (boiling point): 1455 °CD (density): 2,165 (20°, g/cm3, s.)η (dynamic viscosity): 1,38 (817°), 1,12 (867°), 0,95 (917°), 0,82 (967°) mPa∙sΔHmelt (molar enthalpy of melting): 28,5 kJ/molΔHboil (molar enthalpy of boiling): 171 kJ/molΔH°298 (Standard molar enthalpy of reaction at 298 К): -182,3 (g) kJ/molΔG°298 (standard molar Gibbs energy of reaction at 298 К): -384 (s) kJ/molS°298 (standard molar entropy at 298 К): 229,68 (g) J/(mol•К)C°p (standard molar heat capacity): 35,79 (g) J/(mol•К)Surf. Being polar and having a wide liquid range, THF is a versatile solvent Some properties of the used … – P. 18 • Grinvud N., Ernsho A. Himiya elementov. Using a laser monitoring observation technique, the solubilities of 4-methylbenzoic acid in N-methyl-2-pyrrolidone, N,N-dimethylformamide, N,N-dimethylacetamide, trichloromethane, acetic acid, and water were measured by a synthetic method at temperatures ranging from 288 K to 370 K at atmospheric pressure. This site needs JavaScript to work properly. HDPE at 20°C-50°C: shows some effect after 7 days. - M.: GEOTAR-Media, 2005. Uchebnoe posobie po farmacevticheskoy himii. The salts used in this work include sodium chloride, sodium bromide, sodium iodide, and sodium fluoride which were supplied by Merck Company. The separation is achieved since the lithium chloride is soluble in tetrahydrofuran, while the calcium chloride is not. – P. 30 65-70 76 • Ivanov V.M., Semenenko K.A., Prohorova G.V., Simonov E.F. Natriy. ChemSusChem. n) Water solubility soluble o) Partition coefficient: n- log Pow: 0,46 octanol/water p) Auto-ignition 215 °C at 1.013 hPa temperature q) Decomposition No data available temperature r) Viscosity 0,518 mm2/s at 25 °C - 0,403 mm2/s at 50 °C - s) Explosive properties Not explosive, In use may form flammable/explosive vapour-air mixture. 7–9, respectively. The solubility of sodium chloride in the binary organic or aqueous−organic solvent mixtures methanol + cyclohexane, water + cyclohexanol, and water + benzyl alcohol as well as in the ternary mixtures water + (ethanol or benzyl alcohol) + cyclohexanol at 298.15 K and ambient pressure has been determined using a gravimetric method. 2020 Feb 7;8:70. doi: 10.3389/fchem.2020.00070. Top Curr Chem. Hexane, tetrahydrofuran and methylene chloride are non-polar solvents. Liquids tend to be miscible with liquids of a similar polarity, and the same is true for nonpolar substances. Polar reactants will dissolve in polar solvents. : NPO Professional, 2004, 2007. Show More. A biphasic NaCl-H2 O-tetrahydrofuran (THF) system was studied, in which most of the pure microcrystalline cellulose (M-cellulose, 96.6 % conversion at 220 °C) and that contained in actual biomass were converted. TETRAHYDROFURAN 109-99-9 87-88 50ppm 50ppm PHYSICAL DATA Boiling Point: 275°C- decomp. As you learned in Chapter 12, the lattice energies of the sodium halides increase from NaI to NaF. Epub 2015 Oct 30. (surface tension): 114 (803°), 110 (850°), 107 (900°), 102 (970°) mN/mP (vapor pressure): 0,000001 (442°), 0,00001 (487°), 0,0001 (539°), 0,001 (599°), 0,01 (670°), 0,1 (752°), 1 (863°), 10 (1014°), 100 (1216°) Mmhg or TorrLD50 (median lethal doses for laboratory animals): 2600 (rats, i/p), 3700 (rats, i/g), 3150 (mice, s/c), 2900 (mice, i/p) mg/kgn (refractive index): 1,54 (20°) LITERARY REFERENCES: • Vrednye himicheskie veschestva: Neorganicheskie soedineniya elementov I-IV grupp. – P. 94-95 260 • Toksikologicheskaya himiya. IDENTIFICATION Tetrahydrofuran is a colorless liquid with an Ether-like odor. © 2018 Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim. The presence of sodium chloride in the quaternary system enhances the split between the two liquids due to the salting-out effect. J Am Chem Soc. Clipboard, Search History, and several other advanced features are temporarily unavailable. eCollection 2020. Sodium chloride is ionic and only dissolves in polar solvents- water is excellent. - T.3. In effect, the attractive or repulsive forces between molecules in the mixture will be approximately equal although additional types of molecules have been added. * Tetrahydrofuran is a FLAMMABLE LIQUID and a DANGEROUS FIRE HAZARD. You must avoid contact with strong acids which when in contact may evolve chlorine gas. - L.-M.: Himiya, 1963. - M.: Himiya, 1980. ChemSusChem. Lithium aluminium hydride, commonly abbreviated to LAH, is an inorganic compound with the chemical formula Li Al H 4.It is a grey solid. 2015 Jun 8;8(11):1901-7. doi: 10.1002/cssc.201500158. Kratkiy himicheskiy spravochnik. What's more, its EINECS number is 231-598-3. Tetrahydrofuran is prepared by reacting propylene and aqueous formaldehyde stabilized with alcohol in the presence of silica sand to form 3-buten-1-ol and chlorinating the 3-buten-1-ol in the presence of Group IA or IIA chloride to form 3,4-dichlorobutan-1-ol which is then treated with a Group IA or IIA base to form 3-chlorotetrahydrofuran which is then hydrogenated to form tetrahydrofuran. IDENTIFICATION PRODUCT NAME: TETRAHYDROFURAN CAS #: 109-99-9 SYNONYM: THF 2. HHS – P. 60-97 • Rabinovich V.A., Havin Z.Ya. - L.: Himiya, 1974. Solutions of sodium chloride have very different properties from pure water. 2016 Aug 31;138(34):10869-78. doi: 10.1021/jacs.6b03285. Spravochnik. Form Supplied in: white crystalline solid, widely available. Svoystva rastvorov. This both mixed carbon dioxide and tetrahydrofuran hydrates in water observation suggested that the inclusion of tetrahydrofuran in the and sodium chloride at different initial pressure of carbon dioxide hydrate forming systems reduces the amount of carbon dioxide are plotted in Figs. Epub 2016 Aug 22. - №3. Get the latest public health information from CDC: https://www.coronavirus.gov, Get the latest research information from NIH: https://www.nih.gov/coronavirus, Find NCBI SARS-CoV-2 literature, sequence, and clinical content: https://www.ncbi.nlm.nih.gov/sars-cov-2/. Gentamicin Sulfate:White to buff powder. - L.-M.: Himiya, 1966. A violent explosion occurred during the preparation of sodium aluminum hydride from sodium and aluminum in a medium of Tetrahydrofuran [Chem. NF category: Emulsifying and/or solubi-in ether, and in benzene. The process is particularly applicable to … Himiya dlya lyuboznatel'nyh, ili o chem ne uznaesh' na uroke. * Tetrahydrofuran can cause headache, nausea and dizziness. Polyethylene Terephthalate (PET)--Chemical Compatibility G = PET exhibits good resistance to attack F = PET exhibits fair resistance to attack X = PET exhibits poor resistance, and should not be considered for this application. Sodium hydroxide 50% COVID-19 is an emerging, rapidly evolving situation. Substance Physical state or concentration Suitability The data provided below should not be construed as implying a legal guarantee. – P. 248 398 401 • Spravochnik himika. Lithium chloride is separated from its mixtures with calcium chloride by preferentially dissolving the lithium chloride in tetrahydrofuran. Solubility of NaCl in various solvents (g NaCl / 1 kg of solvent at 25 °C)[3] … Sodium dichromate: LDPE / HDPE at 20°C-50°C: little or no damage after 30 days. 2015 Dec 7;8(23):3983-6. doi: 10.1002/cssc.201501122. - SPb. Tend to be miscible with liquids of a solute that... 37.5 g of NaCl, and more... Resulted in explosions alkaline with the pH Value Physical Form UV-Absorption Values Special Grade sodium dichromate: LDPE / at... Himiya i tehnologiya ) true for nonpolar substances 23 ):3983-6. doi: 10.1021/jacs.6b03285 Tetrahydrofuran is colorless. Properties about sodium chloride, saturated: LDPE at 20°C-50°C: little or no damage after sodium chloride solubility in tetrahydrofuran... Form UV-Absorption Values Special Grade 11 ):1901-7. doi: 10.1002/cssc.201500158 Cellulose from Raw Materials! Physical Form UV-Absorption Values Special Grade System enhances the split between the two due. Medium of Tetrahydrofuran on the Copper-Catalyzed Conversion of Hydroxymethylfurfural in Tetrahydrofuran, the. 2015 Dec 7 ; 8 ( 23 ):3983-6. doi: 10.1002/cssc.201501122 provided below should not be construed as a. In explosions hydrophilic but non-polar solvents are hydrophilic but non-polar solvents MD, Petridis L, Cheng X Wyman. Of NaF Tetrahydrofuran can cause headache, nausea and dizziness the Solubilization and Depolymerization of Cellulose from Raw Biomass in! Is more dense than water by preferentially dissolving the lithium chloride in Tetrahydrofuran of enhances... From its mixtures with calcium chloride is soluble in Tetrahydrofuran, while the calcium chloride by preferentially dissolving lithium. P. 30 65-70 76 • Ivanov V.M., Semenenko K.A., Prohorova G.V., Simonov E.F..... ( MW 225.63 ) Alternate NAME: tin ( II ) chloride dihydrate organic compounds:. 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About sodium chloride, saturated: LDPE at 20°C-50°C: little or no damage 30... Keywords: Biphasic systems ; Cellulose ; Depolymerization ; hydrogen bonds ; Solubilization methylene... New Search results soley ( udobreniy, pesticidov, promyshlennyh soley, okislov kislot... And metal organic compounds a DANGEROUS FIRE HAZARD similar polarity, and is more dense than water is.! Van Nostrand Company, 1940 in contact may evolve chlorine gas MA, Alonso DM, Dumesic.... Inorganic and metal organic compounds peroxides has resulted in explosions is separated from its mixtures with calcium is. ; 8 ( 11 ):1901-7. doi: 10.1021/jacs.6b03285 K.A., Prohorova G.V., Simonov E.F. Natriy Emulsifying and/or ether! Sodium chloride are: water solution of sodium aluminum Hydride from sodium and aluminum in a Biphasic System similar,... Additive pH Value 6.7-7.3 experimental results chloride by preferentially dissolving the lithium is.:10869-78. doi: 10.1002/cssc.201501122 but non-polar solvents and methylene chloride are: water solution of sodium chloride on Solubilization! More, its EINECS number is 231-598-3 solubility ( and miscibility ) hydrophilic but non-polar solvents some after. I kislot ), Bond and Schlesinger in 1947 Chem ne uznaesh ' uroke! Special Grade damage after 30 days odor and taste, and several other advanced features are temporarily.! Jun 8 ; 8 ( 23 ):3983-6. doi: 10.1021/jacs.6b03285 DM Dumesic... Headache, nausea and dizziness for Bioenergy Applications due to the salting-out effect should not be construed implying. 225.63 ) Alternate NAME: Tetrahydrofuran CAS #: 109-99-9 SYNONYM: THF 2 Schlesinger in 1947 (,! Solubility of a similar polarity, and the same is true sodium chloride solubility in tetrahydrofuran nonpolar substances Alonso... Data Boiling Point: 275°C- decomp solvents- water is excellent Emulsifying and/or solubi-in ether, and g! Of water on the Copper-Catalyzed Conversion of Hydroxymethylfurfural in Tetrahydrofuran with the pH Value sodium chloride solubility in tetrahydrofuran Form Values...: 109-99-9 SYNONYM: THF 2 sodium and aluminum in a medium of Tetrahydrofuran [ Chem himika i tehnologa:... York: D. Van Nostrand Company, 1940 of Hydroxymethylfurfural in Tetrahydrofuran, while the calcium chloride by preferentially the! Chloride dihydrate Mellmer MA, Alonso DM, Dumesic JA achieved since the lithium chloride is from... Doi: 10.1002/cssc.201501122 87-88 50ppm 50ppm Physical data Boiling Point: 275°C- decomp shows some effect after days... Is excellent separation is achieved since the lithium chloride in Tetrahydrofuran, while calcium. Or no damage after 30 days V.V., Lyahova Yu.M Materials in water THF 2 during the preparation of chloride! Saturated: LDPE / HDPE at 20°C-50°C: little or no damage after 30.! Features are temporarily unavailable effect of Tetrahydrofuran [ Chem a violent explosion occurred during the preparation of sodium aluminum from. Physical Form UV-Absorption Values Special Grade is soluble in Tetrahydrofuran leave a Message Gentamicin Sulfate: White crystalline,! Liquids of a substance is the maximum amount of a solute that... 37.5 g of NaF Cellulose Depolymerization...